SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedin1996,permitseitheretchingorabrading(filing)ofthetestspecimen.ASTME1447"DeterminationofHydrogeninTitaniumandTitaniumAlloysbytheInertGasFusionThermalConductivity/InfraredDetectionMethod"permitssurfacepreparationbyabrading(ifnecessarytoremovecontamination).DifferencesinsamplepreparationpresentsomewhatofadilemmaregardingsimultaneousdeterminationofO,N,andHintitanium.However,abradingsampleswithafiletoremovesurfacecontaminationwillyieldaccurateO,N,andHresults.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.上海禹重實(shí)業(yè)有限公司致力于提供分析儀，竭誠(chéng)為您服務(wù)。LECO分析儀供應(yīng)商

Procedure–Powder/ChipSamplesInstrumentcalibration/driftcorrection.PresstheAnalyzebuttonontheinstrumentscreen.Afterashortdelay,theloadingheadslide-blockwillopen.PlacetheNickelCapsulecontainingthesampleintotheopenportatthetopoftheloadinghead.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodeeithermanuallyorremovethecrucibleandpresstheanalyzebuttontocleanwithanautomaticcleanerifapplicable.LECO分析儀供應(yīng)商上海禹重實(shí)業(yè)有限公司是一家專(zhuān)業(yè)提供分析儀的公司，歡迎新老客戶(hù)來(lái)電！

美國(guó)力可LECO氧氮?dú)浞治鰞x公司介紹：美國(guó)力可公司(LECO)始于1936年，以生產(chǎn)用于冶金、機(jī)械、能源、化工、農(nóng)業(yè)、食品及科研開(kāi)發(fā)領(lǐng)域的各種分析儀器。ONH836氧氣/氮?dú)?氫氣元素分析儀設(shè)計(jì)用于使用惰性氣體熔融技術(shù)對(duì)無(wú)機(jī)材料，鐵和非鐵合金以及耐火材料中的氧，氮和氫含量進(jìn)行寬范圍的測(cè)量。堅(jiān)固的樣品加載區(qū)域可簡(jiǎn)化日常維護(hù)并大程度減少大氣污染用于氧氣檢測(cè)的三重紅外電池可實(shí)現(xiàn)業(yè)內(nèi)大的檢測(cè)范圍通過(guò)自動(dòng)化選項(xiàng)提高實(shí)驗(yàn)室生產(chǎn)率可用的自動(dòng)清潔器大程度地減少了兩次分析之間的手動(dòng)清潔需求適用于坩堝和樣品的20位往復(fù)式裝載機(jī)安裝在動(dòng)臂上的觸摸屏界面可提供更好的人體工程學(xué)設(shè)計(jì)和直觀的操作紅外（IR）和熱導(dǎo)率（TC）檢測(cè)器，沒(méi)有活動(dòng)部件，也無(wú)需手動(dòng)調(diào)節(jié)改善TC電池的穩(wěn)定性可繞過(guò)的OMI-2載氣洗滌塔，提高了TC電池的穩(wěn)定性獲得Dyanamic流量補(bǔ)償可進(jìn)一步增強(qiáng)TC細(xì)胞的穩(wěn)定性

Procedure–Powder/ChipSamplesInstrumentcalibration/driftcorrection.Calibrate/driftfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.AnalyzeSamples.LoginSamplewiththeappropriatenumberofreps.Weighapproximately***gramsofappropriatelypreparedsampleintoa***NickelCapsule,entermassandsampleidentificationintoappropriaterepfields.Ifapplicable,placethenickelcapsuleintheappropriateautoloaderposition.Repeatsteps3cthrough3iforsampleanalysis.上海禹重實(shí)業(yè)有限公司為您提供分析儀，有想法可以來(lái)我司咨詢(xún)！

Instrumentcalibration/driftcorrectionf.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleaner.g.Firmlyplaceagraphitecrucibleonthelowerelectrodetip.h.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically.i.Repeatsteps3bthrough3haminimumofthreetimesforeachcalibration/driftstandardused..Calibrate/driftfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.上海禹重實(shí)業(yè)有限公司是一家專(zhuān)業(yè)提供分析儀的公司，期待您的光臨！LECO分析儀供應(yīng)商

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SamplePreparationSamplingandsamplepreparationofrefractorymetalssuchastitaniumandzirconiumissomewhatdifferentfromthatofsteel.Unlikesteelsamples,hydrogenisnotasmobileinthisgroupofmaterials;therefore,storageinliquidnitrogenordryiceisnotrequired.However,itisimportanttokeepthesamplecoolwhencuttingorsectioning.Samplepreparationforoxygenandnitrogendeterminationhasbeendifferentfromthatofhydrogendetermination.LECO分析儀供應(yīng)商